MOCVD1

The MOCVD1 system includes a cold wall horizontal metalorganic chemical vapor deposition (MOCVD) reactor from CVD Equipment Corp. with an inductively heated SiC-coated graphite susceptor that can accommodate a single wafer up to 2 inches in diameter at temperatures up to 1000 °C. Water circulation through the outer quartz jacket maintains a constant wall temperature. To increase uniformity across the wafer, gas foil rotation of the wafer holder is employed. The reactor loads and unloads through a nitrogen-purged glovebox to minimize exposure to ambient air. The system includes a welded stainless steel gas panel with metal gasket seal fittings, pneumatic valves, mass flow controllers, pressure controllers, etc. that are operated remotely via custom LabView software. Six bubbler manifolds are available for solid or liquid precursors and gas source lines are available for hydrogen selenide and hydrogen sulfide. A separate connection is available for chloride precursors. Purified hydrogen and nitrogen are available as process gases. A chemically resistant rotary vane pump, capacitance manometer, Pirani gauge, throttle valve controller and additional valves are used to maintain reactor pressures in the range from 10-700 Torr.The MOCVD reactor and gas panel are housed in a ventilated enclosure. The gas sources are housed within ventilated gas cabinets and are connected to the main system enclosure via double-walled tubing. An exhaust gas scrubber that includes a pyrolysis stage and a packed tower with sodium hydroxide neutralization system is available to treat the reactor effluents to safe limits. A 16-point Honeywell Vertex M chemcassette system is used to monitor for toxic gases at various points on the system and throughout the lab. The MOCVD system is interlocked with the gas detection unit and other sensors to enable safe shutdown in the event of equipment failure.
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